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Crystal structure of diethyl 3,3'-[(2-fluoro-phen-yl)methyl-idene]bis-(1H-indole-2-carboxyl-ate).

ABSTRACT: In the title compound, C29H25FN2O4, the mean planes of the two indole ring systems (r.m.s. deviations = 0.1392 and 0.0115?Å) are approximately perpendicular to one another, subtending a dihedral angle of 86.0?(5)°; the benzene ring is twisted with respect to the mean planes of the two indole ring systems by 83.3?(2) and 88.1?(4)°, respectively. In the crystal, pairs of N-H?O hydrogen bonds link the mol-ecules into centrosymmetric dimers, which are further linked by N-H?O hydrogen bonds into supra-molecular chains propagating along the [101] direction.

SUBMITTER: Lu XH

PROVIDER: S-EPMC5683515 | biostudies-other | 2017 Nov

REPOSITORIES: biostudies-other

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Crystal structure of diethyl 3,3'-[(2-fluoro-phen-yl)methyl-idene]bis-(1H-indole-2-carboxyl-ate).

Lu Xin-Hua XH Sun Hong-Shun HS Cai Yuan Y Chen Lu-Lu LL Chen Yang-Feng YF

Acta crystallographica. Section E, Crystallographic communications 20171031 Pt 11

In the title compound, C29H25FN2O4, the mean planes of the two indole ring systems (r.m.s. deviations = 0.1392 and 0.0115 Å) are approximately perpendicular to one another, subtending a dihedral angle of 86.0 (5)°; the benzene ring is twisted with respect to the mean planes of the two indole ring systems by 83.3 (2) and 88.1 (4)°, respectively. In the crystal, pairs of N-H⋯O hydrogen bonds link the mol-ecules into centrosymmetric dimers, which are furt ...[more]

PMID: 29152375

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