Unknown

Dataset Information

0

Efficacy of engineered GO Amberlite XAD-16 picolylamine sorbent for the trace determination of Pb (II) and Cu (II) in fishes by solid phase extraction column coupled with inductively coupled plasma optical emission spectrometry.

ABSTRACT: Graphene oxide (GO) was immobilized innovatively through azo spacer arm onto the surface of polymeric Amberlite XAD-16 resin in order to expose all oxygen functionalities freely available for metal ions coordination and further modification with picolylamine which governs selectivity. The GO Amberlite XAD-16 picolylamine enables the development of SPE column coupled with ICP-OES for preconcentration and determination of Pb (II) and Cu (II) in water and fish samples. Elution was performed by mild acid (2M HCl) no other carcinogenic organic solvent was used, prevents ligand leaching. Under optimized conditions, the preconcentration factors of 150 and detection limits 1.434 and 0.048?µg?L-1 for Pb (II) and Cu (II)  were obtained respectively.

SUBMITTER: Javed H 

PROVIDER: S-EPMC6277385 | biostudies-other | 2018 Dec

REPOSITORIES: biostudies-other

Json Xml
altmetric image

Publications

Efficacy of engineered GO Amberlite XAD-16 picolylamine sorbent for the trace determination of Pb (II) and Cu (II) in fishes by solid phase extraction column coupled with inductively coupled plasma optical emission spectrometry.

Javed Hina H   Islam Aminul A   Chauhan Anjali A   Kumar Suneel S   Kumar Sushil S  

Scientific reports 20181203 1

Graphene oxide (GO) was immobilized innovatively through azo spacer arm onto the surface of polymeric Amberlite XAD-16 resin in order to expose all oxygen functionalities freely available for metal ions coordination and further modification with picolylamine which governs selectivity. The GO Amberlite XAD-16 picolylamine enables the development of SPE column coupled with ICP-OES for preconcentration and determination of Pb (II) and Cu (II) in water and fish samples. Elution was performed by mild  ...[more]

Similar Datasets

Unknown Selective solid phase extraction of copper using a new Cu(II)-imprinted polymer and determination by inductively coupled plasma optical emission spectroscopy (ICP-OES).
| S-EPMC3915737 | biostudies-literature
Unknown Mineralisation of atmospheric aerosol particles and further analysis of trace elements by inductively coupled plasma-optical emission spectrometry.
| S-EPMC5480268 | biostudies-literature
Unknown Reusability of SPE and Sb-modified SPE Sensors for Trace Pb(II) Determination.
| S-EPMC6263962 | biostudies-literature
Unknown Preconcentration of Fe(III), Co(II), Ni(II), Cu(II), Zn(II) and Pb(II) with ethylenediamine-modified graphene oxide.
| S-EPMC4701767 | biostudies-literature
Unknown The effect of mustard gas on salivary trace metals (Zn, Mn, Cu, Mg, Mo, Sr, Cd, Ca, Pb, Rb).
| S-EPMC4428796 | biostudies-other
Unknown Polymeric Sorbent Sheets Coupled to Direct Analysis in Real Time Mass Spectrometry for Trace-Level Volatile Analysis-A Multi-Vineyard Evaluation Study.
| S-EPMC7230477 | biostudies-literature
Unknown Mechanical frequency control in inductively coupled electromechanical systems.
| S-EPMC8803975 | biostudies-literature
Unknown Studies on Magnetic and Dielectric Properties of Antiferromagnetically Coupled Dinuclear Cu(II) in a One-Dimensional Cu(II) Coordination Polymer.
| S-EPMC6964276 | biostudies-literature
Unknown Sorption of Cu(II), Zn(II) and Pb(II) Ions in an Aqueous Solution on the PVC-Acetylacetone Composites.
| S-EPMC6473897 | biostudies-other
Unknown Arabidopsis ACBP1 overexpressors are Pb(II)-tolerant and accumulate Pb(II).
| S-EPMC2634561 | biostudies-literature