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Redetermination of Sr2PdO3 from single-crystal X-ray data.


ABSTRACT: The crystal structure redetermination of Sr2PdO3 (distrontium palladium trioxide) was carried out using high-quality single-crystal X-ray data. The Sr2PdO3 structure has been described previously in at least three reports [Wasel-Nielen & Hoppe (1970 ?). Z. Anorg. Allg. Chem. 375, 209-213; Muller & Roy (1971 ?). Adv. Chem. Ser. 98, 28-38; Nagata et al. (2002 ?). J. Alloys Compd. 346, 50-56], all based on powder X-ray diffraction data. The current structure refinement of Sr2PdO3, as compared to previous powder data refinements, leads to more precise cell parameters and fractional coordinates, together with anisotropic displacement parameters for all sites. The compound is confirmed to have the ortho-rhom-bic Sr2CuO3 structure type (space group Immm) as reported previously. The structure consists of infinite chains of corner-sharing PdO4 plaquettes inter-spersed by SrII atoms. A brief comparison of Sr2PdO3 with the related K2NiF4 structure type is given.

SUBMITTER: Thakur GS 

PROVIDER: S-EPMC6323883 | biostudies-other | 2019 Jan

REPOSITORIES: biostudies-other

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Redetermination of Sr<sub>2</sub>PdO<sub>3</sub> from single-crystal X-ray data.

Thakur Gohil S GS   Reuter Hans H   Felser Claudia C   Jansen Martin M  

Acta crystallographica. Section E, Crystallographic communications 20190101 Pt 1


The crystal structure redetermination of Sr<sub>2</sub>PdO<sub>3</sub> (distrontium palladium trioxide) was carried out using high-quality single-crystal X-ray data. The Sr<sub>2</sub>PdO<sub>3</sub> structure has been described previously in at least three reports [Wasel-Nielen & Hoppe (1970 ▸). <i>Z. Anorg. Allg. Chem</i>. <b>375</b>, 209-213; Muller & Roy (1971 ▸). <i>Adv. Chem. Ser</i>. <b>98</b>, 28-38; Nagata <i>et al.</i> (2002 ▸). <i>J. Alloys Compd.</i> <b>346</b>, 50-56], all based on  ...[more]

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