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ABSTRACT:
SUBMITTER: Jansma A
PROVIDER: S-EPMC1395504 | biostudies-literature | 2005 Oct
REPOSITORIES: biostudies-literature
Jansma Ariane A Chuan Tiffany T Albrecht Robert W RW Olson Dean L DL Peck Timothy L TL Geierstanger Bernhard H BH
Analytical chemistry 20051001 19
A microflow CapNMR probe double-tuned for 1H and 13C was installed on a 400-MHz NMR spectrometer and interfaced to an automated liquid handler. Individual samples dissolved in DMSO-d6 are submitted for NMR analysis in vials containing as little as 10 microL of sample. Sets of samples are submitted in a low-volume 384-well plate. Of the 10 microL of sample per well, as with vials, 5 microL is injected into the microflow NMR probe for analysis. For quality control of chemical libraries, 1D NMR spe ...[more]