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(E)-N'-(5-Chloro-2-hydroxy-benzyl-idene)-p-toluene-sulfonohydrazide.

ABSTRACT: The title compound, C(14)H(13)ClN(2)O(3)S, features an intra-molecular O-H?N hydrogen bond which generates an S(6) ring motif. Inter-molecular N-H?O hydrogen bonds and C-H?O close contacts link neighbouring mol-ecules forming R(2) (2)(13) ring motifs. In the crystal structure, mol-ecules are further linked by C-H?Cl inter-actions, forming one-dimensional extended chains along the c axis. The dihedral angle between the two benzene rings is 86.06?(3)°. The crystal structure is further stabilized by weak inter-molecular ?-? inter-actions [inter-planar stacking distance = 3.357?(7)?Å].

SUBMITTER: Kia R 

PROVIDER: S-EPMC2960077 | biostudies-literature | 2008 Nov

REPOSITORIES: biostudies-literature

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(E)-N'-(5-Chloro-2-hydroxy-benzyl-idene)-p-toluene-sulfonohydrazide.

Kia Reza R   Fun Hoong-Kun HK   Kargar Hadi H  

Acta crystallographica. Section E, Structure reports online 20081122 Pt 12

The title compound, C(14)H(13)ClN(2)O(3)S, features an intra-molecular O-H⋯N hydrogen bond which generates an S(6) ring motif. Inter-molecular N-H⋯O hydrogen bonds and C-H⋯O close contacts link neighbouring mol-ecules forming R(2) (2)(13) ring motifs. In the crystal structure, mol-ecules are further linked by C-H⋯Cl inter-actions, forming one-dimensional extended chains along the c axis. The dihedral angle between the two benzene rings is 86.06 (3)°. The crystal structure is further stabilized b  ...[more]

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