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Cytenamide-butyric acid (1/1).

ABSTRACT: Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide-butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol-ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol-ecules are linked by N-H?O and O-H?O hydrogen bonds to form an R(2) (2)(8) heterodimer motif. Pairs of adjacent motifs are further connected via N-H?O inter-actions to form a discrete centrosymmetric assembly.

SUBMITTER: Johnston A

PROVIDER: S-EPMC2961685 | biostudies-literature | 2008 Jun

REPOSITORIES: biostudies-literature

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Cytenamide-butyric acid (1/1).

Johnston Andrea A Florence Alastair J AJ Fabbiani Francesca J A FJ Shankland Kenneth K Bedford Colin T CT

Acta crystallographica. Section E, Structure reports online 20080619 Pt 7

Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide-butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol-ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to form an R(2) (2)(8) heterodimer motif. Pairs of adjacent motifs are further connected via N-H⋯O inter-actions to form a discrete centrosymmetric assembly. ...[more]

PMID: 21202925

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