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2-Fluoro-N-(2-fluoro-benzo-yl)-N-(2-pyrid-yl)benzamide.

ABSTRACT: The title compound, C(19)H(12)F(2)N(2)O(2), a 2:1 product of the reaction of 2-fluoro-benzoyl chloride and 2-amino-pyridine, crystallizes with a disordered 2-fluoro-benzene ring adopting two conformations [ratio of occupancies = 0.930?(4):0.070?(4)] in one of the two independent mol-ecules (differing slightly in conformation) comprising the asymmetric unit. In the crystal structure, C-H?O and C-H??(arene) inter-actions are present.

SUBMITTER: Gallagher JF 

PROVIDER: S-EPMC2968523 | biostudies-literature | 2009 Feb

REPOSITORIES: biostudies-literature

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2-Fluoro-N-(2-fluoro-benzo-yl)-N-(2-pyrid-yl)benzamide.

Gallagher John F JF   Donnelly Katie K   Lough Alan J AJ  

Acta crystallographica. Section E, Structure reports online 20090206 Pt 3

The title compound, C(19)H(12)F(2)N(2)O(2), a 2:1 product of the reaction of 2-fluoro-benzoyl chloride and 2-amino-pyridine, crystallizes with a disordered 2-fluoro-benzene ring adopting two conformations [ratio of occupancies = 0.930 (4):0.070 (4)] in one of the two independent mol-ecules (differing slightly in conformation) comprising the asymmetric unit. In the crystal structure, C-H⋯O and C-H⋯π(arene) inter-actions are present. ...[more]

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