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Bis(benzoyl-acetonato)bis-(1,3-di-4-pyridyl-propane)manganese(II).

ABSTRACT: In the title compound, [Mn(C(10)H(9)O(2))(2)(C(13)H(14)N(2))(2)], the Mn(II) ion lies on a crystallographic inversion center and has a slightly distorted octa-hedral coordination environment. Weak ?-? stacking inter-actions, with centroid-centroid distances of 3.862?(2) and 3.887?(5)?Å, and significant C-H?? inter-actions help to stabilize the crystal structure. The atoms of the unique terminal 4-pyridine-propane group are disordered over two sites, the ratio of refined occpancies being 0.712?(7):0.288?(7).

SUBMITTER: Zhou Y 

PROVIDER: S-EPMC2969015 | biostudies-literature | 2009 Mar

REPOSITORIES: biostudies-literature

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Bis(benzoyl-acetonato)bis-(1,3-di-4-pyridyl-propane)manganese(II).

Zhou Yan Y   Zhao Wen-Na WN   Han Lei L  

Acta crystallographica. Section E, Structure reports online 20090325 Pt 4

In the title compound, [Mn(C(10)H(9)O(2))(2)(C(13)H(14)N(2))(2)], the Mn(II) ion lies on a crystallographic inversion center and has a slightly distorted octa-hedral coordination environment. Weak π-π stacking inter-actions, with centroid-centroid distances of 3.862 (2) and 3.887 (5) Å, and significant C-H⋯π inter-actions help to stabilize the crystal structure. The atoms of the unique terminal 4-pyridine-propane group are disordered over two sites, the ratio of refined occpancies being 0.712 (7  ...[more]

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