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4-(Benzyl-ideneamino)benzene-sulfonamide.


ABSTRACT: The title compound, C(13)H(12)N(2)O(2)S, formed by Schiff base condensation of benzaldehyde with sulfanilamide, crystallizes as discrete mol-ecular species linked by N-H?N and N-H?O hydrogen bonds between the sulfamide nitro-gen H atoms and the aza-methine N and one sulfamide O atom, respectively, forming a two-dimensional array in the bc plane. The aza-methine group is rotated slightly out of the benzaldehyde benzene plane [C-C-C-N torsion angle = 8.1?(3)°], while the dihedral angle between the two benzene rings is 30.0?(1)°.

SUBMITTER: Loughrey BT 

PROVIDER: S-EPMC2970159 | biostudies-literature | 2009 Aug

REPOSITORIES: biostudies-literature

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4-(Benzyl-ideneamino)benzene-sulfonamide.

Loughrey Bradley T BT   Williams Michael L ML   Healy Peter C PC  

Acta crystallographica. Section E, Structure reports online 20090808 Pt 9


The title compound, C(13)H(12)N(2)O(2)S, formed by Schiff base condensation of benzaldehyde with sulfanilamide, crystallizes as discrete mol-ecular species linked by N-H⋯N and N-H⋯O hydrogen bonds between the sulfamide nitro-gen H atoms and the aza-methine N and one sulfamide O atom, respectively, forming a two-dimensional array in the bc plane. The aza-methine group is rotated slightly out of the benzaldehyde benzene plane [C-C-C-N torsion angle = 8.1 (3)°], while the dihedral angle between the  ...[more]

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