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(E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene.

ABSTRACT: The title compound, C(18)H(18)Cl(2)N(2)O(2), was synthesized by the reaction of 1-(5-chloro-2-methoxy-phen-yl)ethanone with hydrazine hydrate. The mol-ecule lies on a crystallographic twofold axis passing through the mid-point of the N-N bond with one half-mol-ecule in the asymmetric unit. The dihedral angle between the two aromatic rings is 44.33?(4)°. In the crystal, inter-molecular C-H?O inter-actions link the mol-ecules into columns along the c axis.

SUBMITTER: Chang JG

PROVIDER: S-EPMC2971795 | biostudies-literature | 2009 Nov

REPOSITORIES: biostudies-literature

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(E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene.

Chang Jian-Guo JG Lu Jie J Zhao Ren-Gao RG

Acta crystallographica. Section E, Structure reports online 20091125 Pt 12

The title compound, C(18)H(18)Cl(2)N(2)O(2), was synthesized by the reaction of 1-(5-chloro-2-methoxy-phen-yl)ethanone with hydrazine hydrate. The mol-ecule lies on a crystallographic twofold axis passing through the mid-point of the N-N bond with one half-mol-ecule in the asymmetric unit. The dihedral angle between the two aromatic rings is 44.33 (4)°. In the crystal, inter-molecular C-H⋯O inter-actions link the mol-ecules into columns along the c axis. ...[more]

PMID: 21578897

Similar Datasets

(μ-3,4-Diacetyl-hexa-2,4-diene-2,5-diol-ato-κO,O:O,O)bis-[aqua(1,10-phen-an-thro-line-κN,N')copper(II)] bis-(tetra-fluorid-oborate) monohydrate.

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