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N'-(3,4-Dihydroxy-benzyl-idene)acetohydrazide monohydrate.

ABSTRACT: In the title compound, C(9)H(10)N(2)O(3)·H(2)O, the Schiff base mol-ecule is approximately planar, the dihedral angle between the benzene and acetohydrazide planes being 5.40?(7)°. An intra-molecular O-H?O hydrogen bond is observed. In the crystal, mol-ecules are linked into a two-dimensional network parallel to (100) by O-H?O, N-H?O, O-H?N and C-H?O hydrogen bonds, and by ?-? inter-actions between symmetry-related benzene rings [centroid-centroid distance = 3.543?(2)?Å].

SUBMITTER: Lv LP 

PROVIDER: S-EPMC2977139 | biostudies-literature | 2009 Jul

REPOSITORIES: biostudies-literature

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N'-(3,4-Dihydroxy-benzyl-idene)acetohydrazide monohydrate.

Lv Lu-Ping LP   Yu Tie-Ming TM   Yu Wen-Bo WB   Li Wei-Wei WW   Hu Xian-Chao XC  

Acta crystallographica. Section E, Structure reports online 20090718 Pt 8

In the title compound, C(9)H(10)N(2)O(3)·H(2)O, the Schiff base mol-ecule is approximately planar, the dihedral angle between the benzene and acetohydrazide planes being 5.40 (7)°. An intra-molecular O-H⋯O hydrogen bond is observed. In the crystal, mol-ecules are linked into a two-dimensional network parallel to (100) by O-H⋯O, N-H⋯O, O-H⋯N and C-H⋯O hydrogen bonds, and by π-π inter-actions between symmetry-related benzene rings [centroid-centroid distance = 3.543 (2) Å]. ...[more]

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