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4-{[(5-Methyl-2-fur-yl)methyl-ene]hydrazinocarbon-yl}pyridinium chloride monohydrate.

ABSTRACT: The title compound, C(12)H(12)N(3)O(2) (+)·Cl(-)·H(2)O, was prepared by the reaction of N'-[(5-methyl-2-fur-yl)methyl-ene]isonicotino-hydrazide and hydro-chloric acid at room temperature. The entire molecule is approximately planar with a maximum deviation of 0.047?(2)?Å. An intramolecular C-H?O interaction is observed. O-H?Cl, N-H?Cl, N-H?O, N-H?N, C-H?Cl and C-H?O hydrogen-bonds stabilize the crystal structure.

SUBMITTER: Li LM

PROVIDER: S-EPMC2977373 | biostudies-literature | 2009 Jul

REPOSITORIES: biostudies-literature

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4-{[(5-Methyl-2-fur-yl)methyl-ene]hydrazinocarbon-yl}pyridinium chloride monohydrate.

Li Li-Min LM Jian Fang-Fang FF Liu Li L

Acta crystallographica. Section E, Structure reports online 20090725 Pt 8

The title compound, C(12)H(12)N(3)O(2) (+)·Cl(-)·H(2)O, was prepared by the reaction of N'-[(5-methyl-2-fur-yl)methyl-ene]isonicotino-hydrazide and hydro-chloric acid at room temperature. The entire molecule is approximately planar with a maximum deviation of 0.047 (2) Å. An intramolecular C-H⋯O interaction is observed. O-H⋯Cl, N-H⋯Cl, N-H⋯O, N-H⋯N, C-H⋯Cl and C-H⋯O hydrogen-bonds stabilize the crystal structure. ...[more]

PMID: 21583659

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