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2,2-Bis(hy-droxy-meth-yl)-2,3-dihydro-1H-pyrrolizin-1-one.

ABSTRACT: The title compound, C(9)H(11)NO(3), was prepared by an Aldol reaction of 2,3-dihydro-1H-pyrrolizin-1-one with formaldehyde. The asymmetric unit contains six mol-ecules. The pyrrolizine ring system in each mol-ecule is planar, the maximum atomic deviation being 0.066?(2)?Å. In the crystal structure, mol-ecules are liked together by an extensive O-H?O hydrogen-bonding network.

SUBMITTER: Ali Y

PROVIDER: S-EPMC3006763 | biostudies-literature | 2010 Jun

REPOSITORIES: biostudies-literature

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2,2-Bis(hy-droxy-meth-yl)-2,3-dihydro-1H-pyrrolizin-1-one.

Ali Yousuf Y Peng Yu Y Hua Erbing E Afza Nighat N Khan Rashid Ali RA

Acta crystallographica. Section E, Structure reports online 20100605 Pt 7

The title compound, C(9)H(11)NO(3), was prepared by an Aldol reaction of 2,3-dihydro-1H-pyrrolizin-1-one with formaldehyde. The asymmetric unit contains six mol-ecules. The pyrrolizine ring system in each mol-ecule is planar, the maximum atomic deviation being 0.066 (2) Å. In the crystal structure, mol-ecules are liked together by an extensive O-H⋯O hydrogen-bonding network. ...[more]

PMID: 21587820

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