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1,2-Bis(benz-yloxy)-1,2-bis-(4-chloro-phen-yl)-3,8-dimeth-oxy-acenaphthene.

ABSTRACT: In the title compound, C(40)H(32)Cl(2)O(4), the two chloro-benzene rings are in syn orientations with respect to the naphthalene ring system and make dihedral angles of 57.12?(6) and 85.74?(6)° with it. The benzene rings of the benz-yloxy group make dihedral angles of 75.34?(6) and 83.95?(7)°, with the naphthalene ring system. In the crystal, the mol-ecules are linked by inter-molecular C-H?Cl inter-actions between the methyl-ene H atoms of the benz-yloxy group and the Cl atoms in adjacent mol-ecules. Furthermore, centrosymmetrically related mol-ecules are linked into dimeric units by pairs of C-H?? inter-actions.

SUBMITTER: Takada T 

PROVIDER: S-EPMC3201419 | biostudies-literature | 2011 Oct

REPOSITORIES: biostudies-literature

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1,2-Bis(benz-yloxy)-1,2-bis-(4-chloro-phen-yl)-3,8-dimeth-oxy-acenaphthene.

Takada Teruhisa T   Hijikata Daichi D   Okamoto Akiko A   Oike Hideaki H   Yonezawa Noriyuki N  

Acta crystallographica. Section E, Structure reports online 20110903 Pt 10

In the title compound, C(40)H(32)Cl(2)O(4), the two chloro-benzene rings are in syn orientations with respect to the naphthalene ring system and make dihedral angles of 57.12 (6) and 85.74 (6)° with it. The benzene rings of the benz-yloxy group make dihedral angles of 75.34 (6) and 83.95 (7)°, with the naphthalene ring system. In the crystal, the mol-ecules are linked by inter-molecular C-H⋯Cl inter-actions between the methyl-ene H atoms of the benz-yloxy group and the Cl atoms in adjacent mol-e  ...[more]

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