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N-(2-Nitro-phenyl-carbamothio-yl)acetamide.

ABSTRACT: In the title compound, C(9)H(9)N(3)O(3)S, the benzene ring and the N-carbamothio-ylacetamide unit are oriented at a dihedral angle of 54.82?(4)°. The dihedral angle between the ring and its attached nitro group is 28.54?(12)°. An intra-molecular, bifurcated N-H?(O,O) hydrogen bond generates two S(6) rings. In the crystal, inversion dimers linked by pairs of N-H?S hydrogen bonds generate R(2) (2)(8) loops. Weak C-H?O inter-actions link the dimers.

SUBMITTER: Shahwar D

PROVIDER: S-EPMC3344673 | biostudies-literature | 2012 May

REPOSITORIES: biostudies-literature

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N-(2-Nitro-phenyl-carbamothio-yl)acetamide.

Shahwar Durre D Tahir M Nawaz MN Chohan Muhammad Mansha MM Khan Muhammad Akmal MA Ahmad Nadeem N

Acta crystallographica. Section E, Structure reports online 20120428 Pt 5

In the title compound, C(9)H(9)N(3)O(3)S, the benzene ring and the N-carbamothio-ylacetamide unit are oriented at a dihedral angle of 54.82 (4)°. The dihedral angle between the ring and its attached nitro group is 28.54 (12)°. An intra-molecular, bifurcated N-H⋯(O,O) hydrogen bond generates two S(6) rings. In the crystal, inversion dimers linked by pairs of N-H⋯S hydrogen bonds generate R(2) (2)(8) loops. Weak C-H⋯O inter-actions link the dimers. ...[more]

PMID: 22590435

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