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1,4-Ditosyl-1,4-diazepane.

ABSTRACT: In the title compound, C(19)H(24)N(2)O(4)S(2), the dihedral angle formed by the benzene rings is 82.88?(7)°, and the mol-ecular conformation is enforced by weak intra-molecular C-H?O contacts. Two C atoms of the 1,4-diazepane ring are disordered over two sets of sites with a refined occupancy ratio of 0.534?(13):0.466?(13). In the crystal, mol-ecules are linked by weak inter-molecular C-H?O inter-actions into chains parallel to the a axis.

SUBMITTER: Yang SH

PROVIDER: S-EPMC3379307 | biostudies-literature | 2012 Jun

REPOSITORIES: biostudies-literature

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1,4-Ditosyl-1,4-diazepane.

Yang Shuang-Hua SH Zhai Zhi-Wei ZW

Acta crystallographica. Section E, Structure reports online 20120512 Pt 6

In the title compound, C(19)H(24)N(2)O(4)S(2), the dihedral angle formed by the benzene rings is 82.88 (7)°, and the mol-ecular conformation is enforced by weak intra-molecular C-H⋯O contacts. Two C atoms of the 1,4-diazepane ring are disordered over two sets of sites with a refined occupancy ratio of 0.534 (13):0.466 (13). In the crystal, mol-ecules are linked by weak inter-molecular C-H⋯O inter-actions into chains parallel to the a axis. ...[more]

PMID: 22719505

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