Unknown

Dataset Information

0

N-Acetyl-5-chloro-3-nitro-l-tyrosine ethyl ester.

ABSTRACT: The title compound, C(13)H(15)ClN(2)O(6), was synthesized by hypochlorous acid-mediated chlorination of N-acetyl-3-nitro-l-tyrosine ethyl ester. The OH group forms an intra-molecular O-H?O hydrogen bond to the nitro group and the N-H group forms an inter-molecular N-H?O hydrogen bonds to an amide O atom, linking the mol-ecules into chains along [100]. The crystal studied was a non-merohedral twin, with a 0.907?(4):0.093?(4) domain ratio.

SUBMITTER: Mutahi TT 

PROVIDER: S-EPMC3435836 | biostudies-literature | 2012 Sep

REPOSITORIES: biostudies-literature

Json Xml
altmetric image

Publications

N-Acetyl-5-chloro-3-nitro-l-tyrosine ethyl ester.

Mutahi Teresa T TT   Edagwa Benson J BJ   Fronczek Frank R FR   Uppu Rao M RM  

Acta crystallographica. Section E, Structure reports online 20120831 Pt 9

The title compound, C(13)H(15)ClN(2)O(6), was synthesized by hypochlorous acid-mediated chlorination of N-acetyl-3-nitro-l-tyrosine ethyl ester. The OH group forms an intra-molecular O-H⋯O hydrogen bond to the nitro group and the N-H group forms an inter-molecular N-H⋯O hydrogen bonds to an amide O atom, linking the mol-ecules into chains along [100]. The crystal studied was a non-merohedral twin, with a 0.907 (4):0.093 (4) domain ratio. ...[more]

Similar Datasets

Unknown Ethyl 4-chloro-3-nitro-benzoate.
| S-EPMC2960261 | biostudies-literature
Unknown 2-Chloro-ethyl 4-nitro-benzoate.
| S-EPMC3009323 | biostudies-literature
Unknown Ethyl 2-acetyl-3-(4-chloro-anilino)butanoate.
| S-EPMC2970076 | biostudies-literature
Unknown (E)-N-(6-Chloro-3-pyridylmeth-yl)-N-ethyl-N'-methyl-2-nitro-ethyl-ene-1,1-diamine.
| S-EPMC2961552 | biostudies-literature
Unknown Ethyl 5-amino-1-(4-chloro-2-nitro-phen-yl)-1H-pyrazole-4-carboxyl-ate.
| S-EPMC2968147 | biostudies-literature
Unknown Ethyl 4-ethyl-amino-3-nitro-benzoate.
| S-EPMC2968249 | biostudies-literature
Unknown Ethyl 3-[7-(N-acetyl-4-meth-oxy-benzene-sulfonamido)-3-chloro-2H-indazol-2-yl]propionate.
| S-EPMC3998507 | biostudies-literature
Unknown Glycine ethyl ester hydro-chloride.
| S-EPMC3007393 | biostudies-literature
Unknown Ethyl 2-{3-[(6-chloro-pyridin-3-yl)meth-yl]-2-(nitro-imino)-imidazolidin-1-yl}acetate.
| S-EPMC3343957 | biostudies-literature
Unknown 3-Acetyl-6-chloro-1-ethyl-4-phenyl-quinolin-2(1H)-one.
| S-EPMC2977505 | biostudies-other