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5-Fluoro-N'-(4-methyl-cyclo-hexyl-idene)-3-phenyl-1H-indole-2-carbohydrazide.

ABSTRACT: The title compound, C22H22FN3O, crystallized with two independent mol-ecules (A and B) in the asymmetric unit; these are linked by a pair of N-H?O hydrogen bonds, forming a pseudo-centrosymmetric dimer with an R (2) 2(10) motif. In addition, a number of C-H?? inter-actions are also observed. The 1H-indole ring systems in mol-ecules A and B are essentially planar [maximum deviations of 0.019?(2) and 0.014?(2)?Å, respectively] and make dihedral angles of 77.64?(10) and 69.50?(9)°, respectively, with thephenyl rings.

SUBMITTER: Celikesir ST

PROVIDER: S-EPMC3793720 | biostudies-literature | 2013

REPOSITORIES: biostudies-literature

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5-Fluoro-N'-(4-methyl-cyclo-hexyl-idene)-3-phenyl-1H-indole-2-carbohydrazide.

Celikesir Sevim Türktekin ST Akkurt Mehmet M Ustündağ Gökçe Cihan GC Capan Gültaze G Büyükgüngör Orhan O

Acta crystallographica. Section E, Structure reports online 20130706 Pt 8

The title compound, C22H22FN3O, crystallized with two independent mol-ecules (A and B) in the asymmetric unit; these are linked by a pair of N-H⋯O hydrogen bonds, forming a pseudo-centrosymmetric dimer with an R (2) 2(10) motif. In addition, a number of C-H⋯π inter-actions are also observed. The 1H-indole ring systems in mol-ecules A and B are essentially planar [maximum deviations of 0.019 (2) and 0.014 (2) Å, respectively] and make dihedral angles of 77.64 (10) and 69.50 (9)°, respectively, wi ...[more]

PMID: 24109307

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