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(3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl-idene)hydrazin-1-yl-idene]indolin-2-one 0.17-hydrate.

ABSTRACT: In the title compound, C16H10N4O2·0.17H2O, prepared by the one-step condensation reaction of isatin with hydrazine hydrate under microwave irradiation, the complete organic mol-ecule is generated by crystallographic inversion symmetry and therefore exists in an S-trans conformation. In the crystal, mol-ecules are linked by N-H?O hydrogen bonds, generating a three-dimensional framework with [001] channels, which are occupied by the disordered water mol-ecules.

SUBMITTER: Liu YH 

PROVIDER: S-EPMC4051016 | biostudies-literature | 2014 Jun

REPOSITORIES: biostudies-literature

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(3Z)-3-[(Z)-2-(2-Oxoindolin-3-yl-idene)hydrazin-1-yl-idene]indolin-2-one 0.17-hydrate.

Liu Yong-Hong YH   Zhao Lei L   Liu Ming-Xuan MX   Lin Hai H   Li Jing-Jing JJ  

Acta crystallographica. Section E, Structure reports online 20140531 Pt 6

In the title compound, C16H10N4O2·0.17H2O, prepared by the one-step condensation reaction of isatin with hydrazine hydrate under microwave irradiation, the complete organic mol-ecule is generated by crystallographic inversion symmetry and therefore exists in an S-trans conformation. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds, generating a three-dimensional framework with [001] channels, which are occupied by the disordered water mol-ecules. ...[more]

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