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Crystal structure of 4-[(E)-(4-nitro-benzyl-idene)amino]-phenol.

ABSTRACT: The asymmetric unit of the title compound, C13H10N2O3, contains four independent mol-ecules (I, II, III and IV). Mol-ecule IV shows whole-mol-ecule disorder over two sets of adjacent sites in a 0.669?(10):0.331?(10) ratio. The dihedral angles between the aromatic rings are 32.30?(13)° in mol-ecule I, 2.24?(14)° in II, 41.61?(13)° in III, 5.0?(5)° in IV (major component) and 10.2?(3)° in IV (minor component). In the crystal, mol-ecules are linked into layers lying parallel to (024) by C-H?O and O-H?O inter-actions. The layers inter-act by C-H?? and weak aromatic ?-? stacking inter-actions [centroid-centroid distances = 3.8476?(16), 3.725?(3) and 3.733?(5)?Å].

SUBMITTER: Atioglu Z 

PROVIDER: S-EPMC4384620 | biostudies-literature | 2015 Feb

REPOSITORIES: biostudies-literature

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Crystal structure of 4-[(E)-(4-nitro-benzyl-idene)amino]-phenol.

Atioğlu Zeliha Z   Akkurt Mehmet M   Jarrahpour Aliasghar A   Ebrahimi Edris E   Büyükgüngör Orhan O  

Acta crystallographica. Section E, Crystallographic communications 20150117 Pt 2

The asymmetric unit of the title compound, C13H10N2O3, contains four independent mol-ecules (I, II, III and IV). Mol-ecule IV shows whole-mol-ecule disorder over two sets of adjacent sites in a 0.669 (10):0.331 (10) ratio. The dihedral angles between the aromatic rings are 32.30 (13)° in mol-ecule I, 2.24 (14)° in II, 41.61 (13)° in III, 5.0 (5)° in IV (major component) and 10.2 (3)° in IV (minor component). In the crystal, mol-ecules are linked into layers lying parallel to (024) by C-H⋯O and O  ...[more]

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