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Crystal structure of 2-nitro-N-(2-nitro-phen-yl)benzamide.

ABSTRACT: In the title compound, C13H9N3O5, the mean plane of the non-H atoms of the central amide fragment C-N-C(=O)-C [r.m.s. deviation = 0.0442?Å] forms dihedral angles of 71.76?(6) and 24.29?(10)° with the C-bonded and N-bonded benzene rings, respectively. In the crystal, mol-ecules are linked by N-H?O hydrogen bonds forming C(4) chains along [100]. Weak C-H?O contacts link the mol-ecules into (100) sheets containing edge-fused R 4 (4)(30) rings. Together, the N-H?O and C-H?O hydrogen bonds generate a three-dimensional network.

SUBMITTER: Moreno-Fuquen R

PROVIDER: S-EPMC4459296 | biostudies-literature | 2015 Jun

REPOSITORIES: biostudies-literature

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Crystal structure of 2-nitro-N-(2-nitro-phen-yl)benzamide.

Moreno-Fuquen Rodolfo R Azcárate Alexis A Kennedy Alan R AR

Acta crystallographica. Section E, Crystallographic communications 20150509 Pt 6

In the title compound, C13H9N3O5, the mean plane of the non-H atoms of the central amide fragment C-N-C(=O)-C [r.m.s. deviation = 0.0442 Å] forms dihedral angles of 71.76 (6) and 24.29 (10)° with the C-bonded and N-bonded benzene rings, respectively. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds forming C(4) chains along [100]. Weak C-H⋯O contacts link the mol-ecules into (100) sheets containing edge-fused R 4 (4)(30) rings. Together, the N-H⋯O and C-H⋯O hydrogen bonds generate a ...[more]

PMID: 26090182

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N-(2-Methyl-phen-yl)-2-nitro-benzamide.

Project description:In the title compound, C(14)H(12)N(2)O(3), the dihedral angle between the two aromatic rings is 41.48 (5)°. The nitro group is twisted by 24.7 (3)° out of the plane of the aromatic ring to which it is attached. The mol-ecules are connected by N-H⋯O hydrogen bonds into chains running along the a axis.

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4-Bromo-N-(2-nitro-phen-yl)benzamide.

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