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Crystal structure of N-(2-amino-5-cyano-4-methyl-sulfanyl-6-oxo-1,6-dihydropyrimidin-1-yl)-4-bromo-benzene-sulfonamide di-methyl-formamide monosolvate.

ABSTRACT: The title compound, C12H10BrN5O3S2·C3H7NO, displays an almost planar amine group. The inter-planar angle between the rings is 31.72?(6)°. The residues are associated into ribbons parallel to [110] by three classical hydrogen bonds; one from each amine Hamine to ODMF and one from NHamide to Ooxo. Adjacent ribbons are connected by translation parallel to the c axis by a 'weak' hydrogen bond Hmeth-yl?Osulfon-yl to form a layer structure parallel to (1-10), while a further contact Hbromo-phen-yl?Osulfon-yl connects the residues in the third dimension.

SUBMITTER: Elgemeie GH

PROVIDER: S-EPMC4645039 | biostudies-literature | 2015 Nov

REPOSITORIES: biostudies-literature

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Crystal structure of N-(2-amino-5-cyano-4-methyl-sulfanyl-6-oxo-1,6-dihydropyrimidin-1-yl)-4-bromo-benzene-sulfonamide di-methyl-formamide monosolvate.

Elgemeie Galal H GH Mohamed Reham A RA Hussein Hoda A HA Jones Peter G PG

Acta crystallographica. Section E, Crystallographic communications 20151014 Pt 11

The title compound, C12H10BrN5O3S2·C3H7NO, displays an almost planar amine group. The inter-planar angle between the rings is 31.72 (6)°. The residues are associated into ribbons parallel to [110] by three classical hydrogen bonds; one from each amine Hamine to ODMF and one from NHamide to Ooxo. Adjacent ribbons are connected by translation parallel to the c axis by a 'weak' hydrogen bond Hmeth-yl⋯Osulfon-yl to form a layer structure parallel to (1-10), while a further contact Hbromo-phen-yl⋯Osu ...[more]

PMID: 26594501

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