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ABSTRACT:
SUBMITTER: Vellas SK
PROVIDER: S-EPMC6290563 | biostudies-literature | 2013 May
REPOSITORIES: biostudies-literature
Vellas Sreedhar K SK Lewis James E M JE Shankar Madhu M Sagatova Alia A Tyndall Joel D A JD Monk Brian C BC Fitchett Christopher M CM Hanton Lyall R LR Crowley James D JD
Molecules (Basel, Switzerland) 20130529 6
A series of metallosupramolecular [Fe₂L₃](BF₄)₄ "click" cylinders have been synthesized in excellent yields (90%-95%) from [Fe(H₂O)₆](BF₄)₂ and bis(bidentate) pyridyl-1,2,3-triazole ligands. All complexes were characterized by elemental analysis, IR, UV-vis, ¹H-, ¹³C- and DOSY-NMR spectroscopies and, in four cases, the structures confirmed by X-ray crystallography. Molecular modeling indicated that some of these "click" complexes were of similar size and shape to related biologically active pyri ...[more]