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Fractal characteristics of shale pore structure and its influence on seepage flow.

ABSTRACT: The migration law of shale gas has a significant influence on the seepage characteristics of shale, and the flow of the gas is closely related to the pore structure. To explore the influence of shale pore parameters on permeability in different diffusion zones, the pore structure of the shale in the Niutitang Formation in Guizhou, China, was analysed based on liquid nitrogen adsorption experiments and nuclear magnetic resonance experiments. The relationship among fractal dimension, organic carbon content (TOC) and BET-specific surface area was analysed based on the fractal dimension of shale pores calculated using the Frenkel-Halsey-Hill model. Shale permeability was calculated using the Knudsen number (Kn) and permeability equation, and the influence of the fractal dimension and porosity in different diffusion zones on shale permeability was analysed. Previous studies have shown that: (i) the pores of shale in the Niutitang Formation, Guizhou are mainly distributed within 1-100 nm, with a small total pore volume per unit mass, average pore diameter, large BET specific surface area and porosity; (ii) fractal dimension has a negative correlation with average pore diameter and TOC content and a quadratic relationship with BET specific surface area; and (iii) permeability has a positive correlation with Kn, porosity and fractal dimension. In the transitional diffusion zone, fractal dimension and porosity have a significant impact on permeability. In the Knudsen diffusion zone, porosity has no obvious effect on permeability. The methodologies and results presented will enable more accurate characterization of the complexity of pore structures of porous media and allow further understanding of the seepage law of shale gas.

SUBMITTER: Wang S

PROVIDER: S-EPMC8131944 | biostudies-literature |

REPOSITORIES: biostudies-literature

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Project description:A multi-functional true triaxial fluid-structure coupling system was used to conduct water retention and seepage tests of shale under true triaxial loading and unloading stress paths. The stress-strain evolution of shale specimens under different experimental conditions was obtained, and the corresponding deformation and strength were analysed. The evolution and failure characteristics of cracks in shale were obtained by CT scanning images before and after the experiment. The results show that the volumetric strain of shale specimen increases first, then decreases and finally continues to increase with an increase in deviatoric stress under water retention, indicating that the volumetric change has experienced a compaction-expansion-compacting. The σ-ε 1 curve of the sample increases first and then decreases, while the deformation in the σ 2 direction shows the repeated compression and expansion. In the seepage test, the permeability-strain curve can be divided into two parts before and after fracture according to the σ-ε 1 curve. Before fracture, the compression velocity of the specimen in the loading direction exceeds the expansion velocity in the unloading direction, resulting in a decrease in volume and a decrease in permeability. With an increase in deviatoric stress, fractures occur inside the particles and continue to spread from the tip until the fractures break through the shale specimen. The pore fissure area increases and the permeability of the sample increases rapidly. In terms of fracture evolution, for the water retention test, dense tensile and shear cracks appear on the failure plane perpendicular to the σ 1 and σ 3 directions, and complex shear fracture network appears on the failure plane perpendicular to the σ 2 direction. For the seepage test, heavy shear failure occurs throughout the original fracture of the sample. With an increase in the penetration depth, the fracture shape on the failure surface perpendicular to the σ 2 direction gradually changes from single to complex.

Project description:The deformation and fracture characteristics of shale in the Changning-Xingwen region were experimentally studied under triaxial cyclic loading with a controlled pore-water pressure. An RLW-2000M microcomputer-controlled coal-rock rheometer was used in the State key Laboratory of coal mine disaster dynamics and control in Chongqing University. These experimental results have indicated the following. (i) The shale softened after being saturated with water, while its failure strength decreased with the increase of axial strain. (ii) A complete cyclic loading-unloading process can be divided into four stages under the coupling action of axial cyclic loading and pore-water pressure; namely the slow or accelerated increasing of strain in the loading stage, and the slow or accelerated decreasing of strain in the unloading stage. (iii) The axial plastic deformation characteristics were similar when pore-water pressures were set to 2, 6 and 10 MPa. Nevertheless, the shale softened ostensibly and fatigue damage occurred during the circulation process when the pore-water pressure was set to 14 MPa. (iv) It has been observed that the mean strain and strain amplitude under axial cyclic are positively correlated with pore-water pressure, while the elastic modulus is negatively correlated with pore-water pressure. As the cycle progresses, the trends in these parameters vary, which indicates that the deformation and elastic characteristics of shale are controlled by pore-water pressure and cyclic loading conditions. (v) Evidenced via triaxial compression tests, it was predominantly shear failure that occurred in the shale specimens. In addition, axial cyclic loading caused the shale to generate complex secondary fractures, resulting in the specimens cracking along the bedding plane due to the effect of pore-water pressure. This study provides valuable insight into the understanding of the deformation and failure mechanisms of shale under complicated stress conditions.

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Fractal characteristics of shale pore structure and its influence on seepage flow.

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