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(E)-5-(3,5-Dimethyl-phen-yl)-N-[4-(methyl-sulfan-yl)benzyl-idene]-1,3,4-thia-diazol-2-amine.

ABSTRACT: The title compound, C(18)H(17)N(3)S(2), was synthesized by the reaction of 5-(3,5-dimethyl-phen-yl)-1,3,4-thia-diazol-2-amine and 4-(methyl-sulfan-yl)benzaldehyde. An intra-molecular C-H?S hydrogen bond results in the formation of a planar (r.m.s. deviation = 0.003?Å) five-membered ring. In the crystal structure, inter-molecular C-H?N hydrogen bonds link the mol-ecules to form layers parallel to (011).

SUBMITTER: Hu J

PROVIDER: S-EPMC2979762 | biostudies-other | 2010

REPOSITORIES: biostudies-other

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(E)-5-(3,5-Dimethyl-phen-yl)-N-[4-(methyl-sulfan-yl)benzyl-idene]-1,3,4-thia-diazol-2-amine.

Hu Jun J Ji Jin-Xiu JX Zhou Ying Y Wang Ji-Kui JK Xu Yan-Hua YH

Acta crystallographica. Section E, Structure reports online 20100120 Pt 2

The title compound, C(18)H(17)N(3)S(2), was synthesized by the reaction of 5-(3,5-dimethyl-phen-yl)-1,3,4-thia-diazol-2-amine and 4-(methyl-sulfan-yl)benzaldehyde. An intra-molecular C-H⋯S hydrogen bond results in the formation of a planar (r.m.s. deviation = 0.003 Å) five-membered ring. In the crystal structure, inter-molecular C-H⋯N hydrogen bonds link the mol-ecules to form layers parallel to (011). ...[more]

PMID: 21579829

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