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1-(2-Nitro-phen-yl)-3-phenyl-thio-urea.

ABSTRACT: The title compound, C(13)H(11)N(3)O(2)S, was prepared by reaction of 2-nitro-benzenamine, KOH and 1-isothio-cyanato-benzene in an ethanol solution at room temperature. The dihedral angles formed between the thiourea plane and the phenyl rings are 61.9 and 31.0°. The dihedral angle between the two phenyl rings is 78.1°. In the crystal structure, there are weak inter-molecular N-H?S and C-H?S hydrogen-bonding inter-actions.

SUBMITTER: Qin Y

PROVIDER: S-EPMC2915211 | biostudies-literature | 2007 Dec

REPOSITORIES: biostudies-literature

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1-(2-Nitro-phen-yl)-3-phenyl-thio-urea.

Qin Yongqi Y Jian Fangfang F Jiang Mingna M Yang Xiangyan X

Acta crystallographica. Section E, Structure reports online 20071206 Pt 1

The title compound, C(13)H(11)N(3)O(2)S, was prepared by reaction of 2-nitro-benzenamine, KOH and 1-isothio-cyanato-benzene in an ethanol solution at room temperature. The dihedral angles formed between the thiourea plane and the phenyl rings are 61.9 and 31.0°. The dihedral angle between the two phenyl rings is 78.1°. In the crystal structure, there are weak inter-molecular N-H⋯S and C-H⋯S hydrogen-bonding inter-actions. ...[more]

PMID: 21200707

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