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N-Phenyl-piperidine-1-carbothio-amide.

ABSTRACT: The title compound, C(12)H(16)N(2)S, was prepared by the reaction of with phenyl isothio-cyanate and piperidine. In the crystal structure, the mol-ecule exhibits inter-molecular N-H?S hydrogen bonds and weak intra-molecular C-H?S and C-H?N hydrogen-bonding inter-actions.

SUBMITTER: Li YF

PROVIDER: S-EPMC2960655 | biostudies-literature | 2008 Aug

REPOSITORIES: biostudies-literature

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N-Phenyl-piperidine-1-carbothio-amide.

Li Yu-Feng YF Jian Fang-Fang FF

Acta crystallographica. Section E, Structure reports online 20080813 Pt 9

The title compound, C(12)H(16)N(2)S, was prepared by the reaction of with phenyl isothio-cyanate and piperidine. In the crystal structure, the mol-ecule exhibits inter-molecular N-H⋯S hydrogen bonds and weak intra-molecular C-H⋯S and C-H⋯N hydrogen-bonding inter-actions. ...[more]

PMID: 21201725

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Project description:In the title compound C(11)H(13)N(3)OS, the aromatic ring and the dihydro-pyrazole ring are oriented orthogonally with respect to each other, making a dihedral angle of 89.92?(9)°. An intra-molecular O-H?S hydrogen bond occurs. In the crystal, weak N-H?N and N-H?S hydrogen bonds link the mol-ecules into a columnar stack propagating along the b axis.

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