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ABSTRACT:
SUBMITTER: Fuller AL
PROVIDER: S-EPMC2961535 | biostudies-literature | 2008 May
REPOSITORIES: biostudies-literature
Acta crystallographica. Section E, Structure reports online 20080503 Pt 6
The title compound, C(10)H(8)BrN, was obtained by slow addition of sodium azide to 8-bromo-1-naphthoic acid, followed by addition of aqueous ammonia. The crude product was crystallized from petroleum ether to give pink crystals. Compared to other 1,8-disubstituted naphthalene compounds, this compound exhibits less strain between the 1 and 8 substituents. Additionally, the NH protons form both intra- and inter-molecular hydrogen bonds. The naphthalene units are arranged in a herring-bone stacking ...[more]