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A second monoclinic polymorph of N-cyclo-hexyl-N-ethyl-benzene-sulfonamide.


ABSTRACT: The crystal structure of the title compound, C(14)H(21)NO(2)S, is a polymorph of the structure reported by Khan et al. [Acta Cryst. (2009), E65, o2867] which is also monoclinic (space group P2(1)/c). The unit cell in the title structure is approximately half the volume of the previously reported polymorph and the asymmetric unit of the title compound contains one mol-ecule rather than two independent mol-ecules in the other polymorph. In the title mol-ecule, the cyclo-hexane ring is in the typical chair form. In the crystal structure, mol-ecules are linked via weak inter-molecular C-H?O inter-actions, forming a chain along the b-axis direction.

SUBMITTER: Haider Z 

PROVIDER: S-EPMC2972150 | biostudies-literature | 2009 Nov

REPOSITORIES: biostudies-literature

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A second monoclinic polymorph of N-cyclo-hexyl-N-ethyl-benzene-sulfonamide.

Haider Zeeshan Z   Arshad Muhammad Nadeem MN   Zia-Ur-Rehman Muhammad M   Khan Islam Ullah IU   Shafiq Muhammad M  

Acta crystallographica. Section E, Structure reports online 20091118 Pt 12


The crystal structure of the title compound, C(14)H(21)NO(2)S, is a polymorph of the structure reported by Khan et al. [Acta Cryst. (2009), E65, o2867] which is also monoclinic (space group P2(1)/c). The unit cell in the title structure is approximately half the volume of the previously reported polymorph and the asymmetric unit of the title compound contains one mol-ecule rather than two independent mol-ecules in the other polymorph. In the title mol-ecule, the cyclo-hexane ring is in the typic  ...[more]

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