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N-Benzoyl-N'-(2-chloro-3-pyrid-yl)thio-urea.

ABSTRACT: The title compound, C(13)H(10)ClN(3)OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothio-cyanate at room temperature. The thio-urea group makes dihedral angles of 47.17?(5) and 51.88?(4)°, respectively, with the benzene and pyridyl rings, while the angle between the benzene and pyridine rings is 8.91?(3)°. Inter-molecular hydrogen-bond inter-actions link neighbouring mol-ecules into an infinite supra-molecular structure.

SUBMITTER: Ding YJ

PROVIDER: S-EPMC2977241 | biostudies-literature | 2009 Jul

REPOSITORIES: biostudies-literature

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N-Benzoyl-N'-(2-chloro-3-pyrid-yl)thio-urea.

Ding Yu-Jie YJ Yao Jian J Wu Jian-Chao JC Dong Wen-Kui WK Tong Jun-Feng JF

Acta crystallographica. Section E, Structure reports online 20090718 Pt 8

The title compound, C(13)H(10)ClN(3)OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothio-cyanate at room temperature. The thio-urea group makes dihedral angles of 47.17 (5) and 51.88 (4)°, respectively, with the benzene and pyridyl rings, while the angle between the benzene and pyridine rings is 8.91 (3)°. Inter-molecular hydrogen-bond inter-actions link neighbouring mol-ecules into an infinite supra-molecular structure. ...[more]

PMID: 21583593

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