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1-Benzoyl-3-(5-quinol-yl)thio-urea.

ABSTRACT: The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio-cyanate and 5-amino-quinoline in the presence of polyethyl-eneglycol-400 (PEG-400)?as a phase-transfer catalyst. The compound crystallized as discrete mol-ecules linked by N-H?N and C-H?N hydrogen bonds involving all the potential donors, generating sheets parallel to (100). An intramolecular N-H?O bond is also present.

SUBMITTER: Du WH

PROVIDER: S-EPMC2968342 | biostudies-literature | 2009 Jan

REPOSITORIES: biostudies-literature

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1-Benzoyl-3-(5-quinol-yl)thio-urea.

Du Wen-Hu WH Wei Chang-Mei CM Wang Wei-Feng WF

Acta crystallographica. Section E, Structure reports online 20090114 Pt 2

The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio-cyanate and 5-amino-quinoline in the presence of polyethyl-eneglycol-400 (PEG-400) as a phase-transfer catalyst. The compound crystallized as discrete mol-ecules linked by N-H⋯N and C-H⋯N hydrogen bonds involving all the potential donors, generating sheets parallel to (100). An intramolecular N-H⋯O bond is also present. ...[more]

PMID: 21581917

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