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12,12'-[2,2'-Oxybis(ethane-2,1-di-yl)bis-(-oxy)]bis-[(R(p))-4-bromo-[2.2]paracyclo-phane].

ABSTRACT: The title compound, C(36)H(36)Br(2)O(3), was synthesized from (R(p))-4-bromo-12-hy-droxy[2.2]paracyclo-phane and oxydiethane-2,1-diyl bis-(4-methyl-benzene-sulfonate). The crystal packing exhibits a short O?Br inter-action [Br?O = 3.185?(3)?Å] and a weak inter-molecular C-H?O contact.

SUBMITTER: Hong B

PROVIDER: S-EPMC3100051 | biostudies-literature | 2011 Apr

REPOSITORIES: biostudies-literature

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12,12'-[2,2'-Oxybis(ethane-2,1-di-yl)bis-(-oxy)]bis-[(R(p))-4-bromo-[2.2]paracyclo-phane].

Hong Bing B Ma Yudao Y Duan Wenzeng W He Fuyan F Zhao Lei L

Acta crystallographica. Section E, Structure reports online 20110323 Pt 4

The title compound, C(36)H(36)Br(2)O(3), was synthesized from (R(p))-4-bromo-12-hy-droxy[2.2]paracyclo-phane and oxydiethane-2,1-diyl bis-(4-methyl-benzene-sulfonate). The crystal packing exhibits a short O⋯Br inter-action [Br⋯O = 3.185 (3) Å] and a weak inter-molecular C-H⋯O contact. ...[more]

PMID: 21754216

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