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(E)-1-(2-Hy-droxy-5-meth-oxy-benzyl-idene)thio-semicarbazide.

ABSTRACT: In the title mol-ecule, C(9)H(11)N(3)O(2)S, an intra-molecular O-H?N hydrogen bond generates an S(6) ring motif. In the crystal, mol-ecules are linked via pairs of N-H?S inter-actions, forming inversion dimers with R(2) (2)(8) ring motifs. These dimers are further linked via N-H?S and N-H?O hydrogen bonds, forming a two-dimensional network lying parallel to (100). The crystal structure is further stabilized by inter-molecular ?-? inter-actions [centroid-centroid distance = 3.7972?(9)?Å].

SUBMITTER: Adabi Ardakani A 

PROVIDER: S-EPMC3275013 | biostudies-literature | 2012 Feb

REPOSITORIES: biostudies-literature

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(E)-1-(2-Hy-droxy-5-meth-oxy-benzyl-idene)thio-semicarbazide.

Adabi Ardakani Amir A   Kargar Hadi H   Kia Reza R   Tahir Muhammad Nawaz MN  

Acta crystallographica. Section E, Structure reports online 20120111 Pt 2

In the title mol-ecule, C(9)H(11)N(3)O(2)S, an intra-molecular O-H⋯N hydrogen bond generates an S(6) ring motif. In the crystal, mol-ecules are linked via pairs of N-H⋯S inter-actions, forming inversion dimers with R(2) (2)(8) ring motifs. These dimers are further linked via N-H⋯S and N-H⋯O hydrogen bonds, forming a two-dimensional network lying parallel to (100). The crystal structure is further stabilized by inter-molecular π-π inter-actions [centroid-centroid distance = 3.7972 (9) Å]. ...[more]

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