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(E)-4-Bromo-N'-(4-hy-droxy-3-meth-oxy-benzyl-idene)benzohydrazide monohydrate.

ABSTRACT: In the title compound, C(15)H(13)BrN(2)O(3)·H(2)O, the dihedral angle between the two benzene rings is 13.92?(6)°. The meth-oxy group of the 4-hy-droxy-3-meth-oxy-phenyl is almost coplanar with its bound benzene ring, as seen by the C(meth-yl)-O-C-C torsion angle of -0.35?(16)°. In the crystal, mol-ecules are linked into a three-dimensional network by N-H?O, O-H?N and O-H?O hydrogen bonds and also weak C-H?O inter-actions. A short C?O contact of 3.0191?(15)?Å is also present.

SUBMITTER: Horkaew J 

PROVIDER: S-EPMC3344027 | biostudies-literature | 2012 Apr

REPOSITORIES: biostudies-literature

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(E)-4-Bromo-N'-(4-hy-droxy-3-meth-oxy-benzyl-idene)benzohydrazide monohydrate.

Horkaew Jirapa J   Chantrapromma Suchada S   Anantapong Teerasak T   Kanjana-Opas Akkharawit A   Fun Hoong-Kun HK  

Acta crystallographica. Section E, Structure reports online 20120314 Pt 4

In the title compound, C(15)H(13)BrN(2)O(3)·H(2)O, the dihedral angle between the two benzene rings is 13.92 (6)°. The meth-oxy group of the 4-hy-droxy-3-meth-oxy-phenyl is almost coplanar with its bound benzene ring, as seen by the C(meth-yl)-O-C-C torsion angle of -0.35 (16)°. In the crystal, mol-ecules are linked into a three-dimensional network by N-H⋯O, O-H⋯N and O-H⋯O hydrogen bonds and also weak C-H⋯O inter-actions. A short C⋯O contact of 3.0191 (15) Å is also present. ...[more]

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