Unknown

Dataset Information

0

1,3,5-Tri-p-tolyl-pentane-1,5-diol.

ABSTRACT: In the title compound, C26H30O2, the central benzene ring forms dihedral angles of 14.85?(15) and 28.17?(14)° with the terminal benzene rings. The dihedral angle between the terminal benzene rings is 32.14?(13)°. The crystal packing exhibits two strong inter-molecular O-H?O hydrogen bonds, forming directed four-membered co-operative rings. A region of disordered electron density, most probably disordered ethyl acetate solvent mol-ecules, occupying voids of ca 519?Å(3) for an electron count of 59, was treated using the SQUEEZE routine in PLATON [Spek (2009 ?). Acta Cryst. D65, 148-155]. Their formula mass and unit-cell characteristics were not taken into account during refinement. The structure was refined as an inversion twin [absolute structure parameter = -0.3?(4)].

SUBMITTER: Thiruvalluvar A 

PROVIDER: S-EPMC3998290 | biostudies-literature | 2014 Feb

REPOSITORIES: biostudies-literature

Json Xml
altmetric image

Publications

1,3,5-Tri-p-tolyl-pentane-1,5-diol.

Thiruvalluvar A A   Chithiravel R R   Muthusubramanian S S   Butcher R J RJ  

Acta crystallographica. Section E, Structure reports online 20140111 Pt 2

In the title compound, C26H30O2, the central benzene ring forms dihedral angles of 14.85 (15) and 28.17 (14)° with the terminal benzene rings. The dihedral angle between the terminal benzene rings is 32.14 (13)°. The crystal packing exhibits two strong inter-molecular O-H⋯O hydrogen bonds, forming directed four-membered co-operative rings. A region of disordered electron density, most probably disordered ethyl acetate solvent mol-ecules, occupying voids of ca 519 Å(3) for an electron count of 59  ...[more]

Similar Datasets

Unknown 1,3,5-Tri-p-tolyl-pentane-1,5-dione.
| S-EPMC2959968 | biostudies-literature
Unknown 1,5-Dimethyl-2-nitro-imino-1,3,5-tri-azinane.
| S-EPMC2962141 | biostudies-literature
Unknown Tri-p-tolyl-phosphine.
| S-EPMC2960611 | biostudies-literature
Unknown 1,1,1,5,5,5-Hexafluoro-2,4-dimeth-oxy-pentane-2,4-diol.
| S-EPMC3238828 | biostudies-literature
Unknown 2,4,6-Tri-p-tolyl-pyridine.
| S-EPMC2969604 | biostudies-literature
Unknown Pentane-1,5-diammonium tetra-chlorido-palladate(II).
| S-EPMC2915137 | biostudies-literature
Unknown 3-(3-Bromo-4-methoxy-phen-yl)-1,5-diphenyl-pentane-1,5-dione.
| S-EPMC2984057 | biostudies-literature
Unknown 1,5-Bis(4-chloro-phen-yl)-3-(2-thien-yl)pentane-1,5-dione.
| S-EPMC2959928 | biostudies-literature
Unknown 1,3,5-Tri-fluoro-2,4,6-tri-iodo-benzene-piperazine (2/1).
| S-EPMC9462296 | biostudies-literature
Unknown 1,5-Bis(4-bromo-phen-yl)-3-phenyl-pentane-1,5-dione.
| S-EPMC2960541 | biostudies-other