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Bonding of resin cement to zirconia with high pressure primer coating.

ABSTRACT: OBJECTIVES: To investigate the effect of air-drying pressure during ceramic primer coating on zirconia/resin bonding and the surface characteristics of the primed zirconia. METHODS: Two ceramic primers (Clearfil Ceramic Primer, CCP, Kuraray Medical Inc. and Z-Prime Plus, ZPP, Bisco Inc.) were applied on the surface of air-abraded zirconia (Katana zirconia, Noritake) and dried at 4 different air pressures (0.1-0.4 MPa). The primed zirconia ceramic specimens were bonded with a resin-based luting agent (SA Luting Cement, Kuraray). Micro-shear bond strengths of the bonded specimens were tested after 3 days of water storage or 5,000× thermocycling (n = 12). Failure modes of the fractured specimens were examined with scanning electron miscopy. The effects of air pressure on the thickness of the primer layers and the surface roughness (Sa) of primed zirconia were evaluated using spectroscopic ellipsometry (n = 6), optical profilometry and environmental scanning electron microscopy (ESEM) (n = 6), respectively. RESULTS: Clearfil Ceramic Primer air-dried at 0.3 and 0.4 MPa, yielding significantly higher µSBS than gentle air-drying subgroups (p < 0.05). Compared to vigorous drying conditions, Z-Prime Plus air-dried at 0.2 MPa exhibited significantly higher µSBS (p < 0.05). Increasing air-drying pressure reduced the film thickness for both primers. Profilometry measurements and ESEM showed rougher surfaces in the high pressure subgroups of CCP and intermediate pressure subgroup of ZPP. CONCLUSION: Air-drying pressure influences resin/zirconia bond strength and durability significantly. Higher air-drying pressure (0.3-0.4 MPa) for CCP and intermediate pressure (0.2 MPa) for ZPP are recommended to produce strong, durable bonds between resin cement and zirconia ceramics.

SUBMITTER: Wang C

PROVIDER: S-EPMC4081122 | biostudies-literature | 2014

REPOSITORIES: biostudies-literature

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Bonding of resin cement to zirconia with high pressure primer coating.

Wang Chen C Niu Li-na LN Wang Ying-jie YJ Jiao Kai K Liu Yan Y Zhou Wei W Shen Li-juan LJ Fang Ming M Li Meng M Zhang Xiang X Tay Franklin R FR Chen Ji-hua JH

PloS one 20140703 7

<h4>Objectives</h4>To investigate the effect of air-drying pressure during ceramic primer coating on zirconia/resin bonding and the surface characteristics of the primed zirconia.<h4>Methods</h4>Two ceramic primers (Clearfil Ceramic Primer, CCP, Kuraray Medical Inc. and Z-Prime Plus, ZPP, Bisco Inc.) were applied on the surface of air-abraded zirconia (Katana zirconia, Noritake) and dried at 4 different air pressures (0.1-0.4 MPa). The primed zirconia ceramic specimens were bonded with a resin-b ...[more]

PMID: 24992678

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Project description:BackgroundTo evaluate the effects of four ceramic primers and two cement types on the bonding strength and durability between zirconia and resin cement.MethodsA total of 115 polished and air-abraded zirconia blocks were randomly divided into five groups (with 23 in each group) to test the performance of various primers. Meanwhile, all primer samples were divided into two subgroups randomly to measure the difference between the two cement types. Group No treat - Clearfil SA Cement (NT-C); group No treat - RelyX Unicem Cement (NT-U); group Z-Prime Plus - Clearfil SA Cement (ZPP-C); group Z-Prime Plus - RelyX Unicem Cement (ZPP-U); group Rely X Ceramic Primer - Clearfil SA Cement (RCP-C); group Rely X Ceramic Primer - RelyX Unicem Cement (RCP-U); group Clearfil Ceramic Primer - Clearfil SA Cement (CCP-C); group Clearfil Ceramic Primer - RelyX Unicem Cement (CCP-U); group Monobond-S - Clearfil SA Cement (MS-C); group Monobond-S - RelyX Unicem Cement (MS-U). According to the type of cement, the specimens were randomly selected for electron microscope scanning and energy spectrum analysis, and the tightness of zirconium porcelain resin adhesive interface was observed. The bonding strength of different adhesives and aging experiments were tested by shear test mode, and the shear strength of each experimental group was analyzed by one variable three factor analysis of variance.ResultsAll primers in the treated groups maintained a pristine structure without micro-crack, while the non-primer treatment sample exhibited obvious micro-cracks. Furthermore, among the four primers, the sample treated with Clearfil Ceramic Primer (CCP) obtained the highest bonding strength, with a statistically significant difference (P<0.05). However, cohesive failure mainly occurred in the CCP group before thermal cycles, and mixed failure occurred after thermal cycles.ConclusionsCCP is the superior primer, and can improve the bonding strength between zirconia and resin cement. Because the thermal cycles have a significantly adverse effect on the shear bond strength, CCP can be helpful in improving the durability of the zirconia bonding strength. Furthermore, the two cement types exhibited a similar bonding performance for zirconia.

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Bonding of resin cement to zirconia with high pressure primer coating.

Publications

Bonding of resin cement to zirconia with high pressure primer coating.

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