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A study of the effects of synthesis conditions on Li5FeO4/carbon nanotube composites.


ABSTRACT: Li5FeO4/carbon nanotube (LFO/CNT) composites composed of sub-micron sized LFO and a nanocarbon with high electrical conductivity were successfully synthesized for the use as lithium ion predoping source in lithium ion cells. The phase of LFO in the composite was found to be very sensitive to the synthesis conditions, such as the heat treatment temperature, type of lithium salt, and physical state of the precursors (powder or pellet), due to the carbothermic reduction of Fe3O4 by CNTs during high temperature solid state reaction. Under optimized synthesis conditions, LFO/CNT composites could be synthesized without the formation of impurities. To the best of our knowledge, this is the first report on the synthesis and characterization of a sub-micron sized LFO/CNT composites.

SUBMITTER: Lee SW 

PROVIDER: S-EPMC5396188 | biostudies-literature | 2017 Apr

REPOSITORIES: biostudies-literature

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A study of the effects of synthesis conditions on Li<sub>5</sub>FeO<sub>4</sub>/carbon nanotube composites.

Lee Suk-Woo SW   Kim Hyun-Kyung HK   Kim Myeong-Seong MS   Roh Kwang Chul KC   Kim Kwang-Bum KB  

Scientific reports 20170419


Li<sub>5</sub>FeO<sub>4</sub>/carbon nanotube (LFO/CNT) composites composed of sub-micron sized LFO and a nanocarbon with high electrical conductivity were successfully synthesized for the use as lithium ion predoping source in lithium ion cells. The phase of LFO in the composite was found to be very sensitive to the synthesis conditions, such as the heat treatment temperature, type of lithium salt, and physical state of the precursors (powder or pellet), due to the carbothermic reduction of Fe<  ...[more]

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