Browse
Submit Data
Databases
API
Help

Dataset Information

20 Views

0 Connections

0 Citations

0 Reanalyses

0 Downloads

Omics score: 0

Precipitation during Quenching in 2A97 Aluminum Alloy and the Influences from Grain Structure.

ABSTRACT: The quench-induced precipitation and subsequent aging response in 2A97 aluminum alloy was investigated based on the systematic microstructure characterization. Specifically, the influence on precipitation from grain structure was examined. The results indicated the evident influence from the cooling rate of the quenching process. Precipitation of T₁ and δ' phase can hardly occur in the specimen exposed to water quenching while become noticeable in the case of air cooling. The yield strength of 2A97-T6 alloy de-graded by 234 MPa along with a comparable elongation when water quenching was replaced by air cooling. Sub-grains exhibited a much higher sensitivity to the precipitation during quenching. The presence of dislocations in sub-grains promoted the quench-induced precipitation by acting as nucleation sites and enhancing the diffusion of the solute. A quenching rate of 3 °C/s is tolerable for recrystallized grains in 2A97 Al alloy but is inadequate for sub-grains to inhibit precipitation. The study fosters the feasibility of alleviating quench-induced precipitation through cultivating the recrystallization structure in highly alloyed Al-Cu-Li alloys.

SUBMITTER: Wang X

PROVIDER: S-EPMC8197508 | biostudies-literature |

REPOSITORIES: biostudies-literature

ACCESS DATA

Json Xml

Similar Datasets

Grain Refinement Mechanism of 5A06 Aluminum Alloy Sheets during Cold Rotary Forging.

Project description:This paper studies the grain refinement mechanisms of 5A06 aluminum alloy sheets in cold rotary forging (CRF). The results show that the grains are clearly refined from 25.1 µm to 11.8 µm during the CRF process. The grain refinement mechanism can be divided into two modes: (1) The grains with a small Schmid factor (SF) are activated by multi-slip systems, and dense dislocations are segregated along the boundaries of interior regions with different slip systems, which results in a rapidly increasing strain localization along these boundaries. Since the strain localization restrains the coordinate slip deformation between different interior regions, the grains are directly separated into several finer grains. (2) The grains with a large SF are primarily activated by a single slip system, and the dislocation migrates smoothly along most microband boundaries. Then, a more severe lattice rotation causes a transformation to a hard orientation and multi-slip system activation, which contributes to an increase in the rapid misorientation across microband boundaries and thus promotes significant SF grain refinement.

| S-EPMC10096004 | biostudies-literature

Precipitation of a new platelet phase during the quenching of an Al-Zn-Mg-Cu alloy.

Project description:A previously undescribed high aspect ratio strengthening platelet phase, herein named the Y-phase, has been identified in a commercial Al-Zn-Mg-Cu alloy. Differential scanning calorimetry indicates that this phase only precipitates at temperature and cooling rate of about 150-250 °C and 0.05-300 K/s, respectively. This precipitate is shown to be responsible for a noticeable improvement in mechanical properties. Aberration corrected scanning transmission electron microscopy demonstrates the minimal thickness (~1.4 nm) precipitate plates are isostructural to those of the T1 (Al2CuLi) phase observed in Al-Cu-Li alloys. Low voltage chemical analysis by energy dispersive X-ray spectroscopy and electron energy loss spectroscopy gives evidence of the spatial partitioning of the Al, Cu and Zn within the Y-phase, as well as demonstrating the incorporation of a small amount of Mg.

| S-EPMC4793252 | biostudies-literature

Effect of Grain Structure and Quenching Rate on the Susceptibility to Exfoliation Corrosion in 7085 Alloy.

Project description:The influence of grain structure and quenching rates on the exfoliation corrosion (EXCO) susceptibility of 7085 alloy was studied using immersion tests, optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and scanning transmission electron microscopy (STEM). The results show that as the cooling rate decreases from 1048 °C/min to 129 °C/min; the size of grain boundary precipitates (GBPs); the width of precipitate-free zones (PFZ); and the content of Zn, Mg, and Cu in GBPs rise, leading to an increase in EXCO depth and consequently higher EXCO susceptibility. Meanwhile, there is a linear relationship between the average corrosion depth and the logarithm of the cooling rate. Corrosion cracks initiate at the grain boundaries (GBs) and primarily propagate along the HAGBs. In the bar grain (BG) sample at lower cooling rates, crack propagation along the sub-grain boundaries (SGBs) was observed. Compared to equiaxed grain (EG) samples, the elongated grain samples exhibit larger GBPs, a wider PFZ, and minor compositional differences in the GBPs, resulting in higher EXCO susceptibility.

| S-EPMC10574189 | biostudies-literature

The Microstructure Evolution and Electrochemical Corrosion Behavior of 7A46 Aluminum Alloy in Different Quenching Conditions.

Project description:The quenching condition of aluminum alloy can affect the mechanical property and corrosion resistance of the profile. This paper is aimed at the low quench sensitivity of aluminum alloys. Scanning electron microscopy and transmission electron microscopy were used to analyze precipitate behaviors of the 7A46 aluminum alloy under different isothermal cooling conditions and microstructure evolutions of quench-induced precipitations. The effect of the different isothermal time on the corrosion resistance of the alloy, and the relationship between microstructure and corrosion resistance after quenching were revealed through electrochemical impedance spectroscopy and potentiodynamic polarization tests. Results show that corrosion sensitivity of the quenching-aged alloy is much higher than that of the double-aged (DA) alloy, and the corrosion resistance of the quenched alloy decreases firstly and then increases. Due to the high density of the matrix precipitates, the increased content of the impurity element, the discontinuity of the grain boundary precipitates and the widening of the precipitates free zone, the most serious degree of corrosion performance among the quenched alloys is 295 °C at 800 s, and the self-corrosion potential and self-current density is -0.919 V and 2.371 μA/cm2, respectively.

| S-EPMC8777919 | biostudies-literature

The Dependence of Isothermal ω Precipitation on the Quenching Rate in a Metastable β-Ti Alloy.

Project description:The precipitation behavior of the α strengthening phase in metastable β-Ti alloys is highly dependent on heat treatment parameters such as quenching rate, heating rate and ageing temperature. In this paper we have investigated the influence of quenching rate on the formation of isothermal ω precipitates that have been regarded as potent nucleant sites for α precipitation. The results show that the β-solutionized alloy contains a β matrix with a layer structured morphology. Regular atomic movement of the (002)β plane along the <002> direction was observed in the alloy. The increase in quenching rate refines the thickness of layers, subsequently influencing the nucleation and growth of isothermal ω precipitates after ageing treatment. The high quenching rate promotes the occurrence of ω precipitation, broadens the stage of ω precipitation and increases the number density of ω precipitates. Since the isothermal ω phase provides a heterogeneous nucleation site for α precipitates, it is inferred that the quenching rate may indirectly influence the mechanical properties of metastable β-Ti alloy.

| S-EPMC4598871 | biostudies-other

Isothermal Time-Temperature-Precipitation Diagram for an Aluminum Alloy 6005A by In Situ DSC Experiments.

Project description:Time-temperature-precipitation (TTP) diagrams deliver important material data, such as temperature and time ranges critical for precipitation during the quenching step of the age hardening procedure. Although the quenching step is continuous, isothermal TTP diagrams are often applied. Together with a so-called Quench Factor Analysis, they can be used to describe very different cooling paths. Typically, these diagrams are constructed based on mechanical properties or microstructures after an interrupted quenching, i.e., ex situ analyses. In recent years, an in situ calorimetric method to record continuous cooling precipitation diagrams of aluminum alloys has been developed to the application level by our group. This method has now been transferred to isothermal experiments, in which the whole heat treatment cycle was performed in a differential scanning calorimeter. The Al-Mg-Si-wrought alloy 6005A was investigated. Solution annealing at 540 °C and overcritical quenching to several temperatures between 450 °C and 250 °C were followed by isothermal soaking. Based on the heat flow curves during isothermal soaking, TTP diagrams were determined. An appropriate evaluation method has been developed. It was found that three different precipitation reactions in characteristic temperature intervals exist. Some of the low temperature reactions are not accessible in continuous cooling experiments and require isothermal studies.

| S-EPMC5453356 | biostudies-other

Aluminum-copper alloy anode materials for high-energy aqueous aluminum batteries.

Project description:Aqueous aluminum batteries are promising post-lithium battery technologies for large-scale energy storage applications because of the raw materials abundance, low costs, safety and high theoretical capacity. However, their development is hindered by the unsatisfactory electrochemical behaviour of the Al metal electrode due to the presence of an oxide layer and hydrogen side reaction. To circumvent these issues, we report aluminum-copper alloy lamellar heterostructures as anode active materials. These alloys improve the Al-ion electrochemical reversibility (e.g., achieving dendrite-free Al deposition during stripping/plating cycles) by using periodic galvanic couplings of alternating anodic α-aluminum and cathodic intermetallic Al2Cu nanometric lamellas. In symmetric cell configuration with a low oxygen concentration (i.e., 0.13 mg L-1) aqueous electrolyte solution, the lamella-nanostructured eutectic Al82Cu18 alloy electrode allows Al stripping/plating for 2000 h with an overpotential lower than ±53 mV. When the Al82Cu18 anode is tested in combination with an AlxMnO2 cathode material, the aqueous full cell delivers specific energy of ~670 Wh kg-1 at 100 mA g-1 and an initial discharge capacity of ~400 mAh g-1 at 500 mA g-1 with a capacity retention of 83% after 400 cycles.

| S-EPMC8803968 | biostudies-literature

Precipitation strengthening in an ultralight magnesium alloy.

Project description:Body-centred cubic magnesium-lithium-aluminium-base alloys are the lightest of all the structural alloys, with recently developed alloy compositions showing a unique multi-dimensional property profile. By hitherto unrecognised mechanisms, such alloys also exhibit exceptional immediate strengthening after solution treatment and water quenching, but strength eventually decreases during prolonged low temperature ageing. We show that such phenomena are due to the precipitation of semi-coherent D03-Mg3Al nanoparticles during rapid cooling followed by gradual coarsening and subsequent loss of coherency. Physical explanation of these phenomena allowed the creation of an exceptionally low-density alloy that is also structurally stable by controlling the lattice mismatch and volume fraction of the Mg3Al nanoparticles. The outcome is one of highest specific-strength engineering alloys ever developed.

| S-EPMC6397269 | biostudies-literature

Direct observation of grain rotations during coarsening of a semisolid Al-Cu alloy.

Project description:Sintering is a key technology for processing ceramic and metallic powders into solid objects of complex geometry, particularly in the burgeoning field of energy storage materials. The modeling of sintering processes, however, has not kept pace with applications. Conventional models, which assume ideal arrangements of constituent powders while ignoring their underlying crystallinity, achieve at best a qualitative description of the rearrangement, densification, and coarsening of powder compacts during thermal processing. Treating a semisolid Al-Cu alloy as a model system for late-stage sintering-during which densification plays a subordinate role to coarsening-we have used 3D X-ray diffraction microscopy to track the changes in sample microstructure induced by annealing. The results establish the occurrence of significant particle rotations, driven in part by the dependence of boundary energy on crystallographic misorientation. Evidently, a comprehensive model for sintering must incorporate crystallographic parameters into the thermodynamic driving forces governing microstructural evolution.

| S-EPMC5068287 | biostudies-literature

Analysis of Incremental Sheet Forming of Aluminum Alloy.

Project description:Recent developments in incremental sheet forming have resulted in the creation of novel manufacturing processes that are highly adaptable and could bring significant economic benefits for advanced technologies and low-volume production. In this manuscript, the following variables were examined: the variation in the deformation forces for a part with a pyramidal trunk shape; the variation in the deformations and thinning of the Al 3003 material during the incremental forming process; and the variation in the accuracy of the incrementally formed part and the quality of the surfaces (surface roughness). The components of the forces in the incremental forming have increasing values from the beginning of the process to the maximum value due to the hardening process. The TiN-coated tool ensures lower values of the forming components. Due to the kinematics of the forming process, deviations, especially in shape, from the part in the drawing are observed, which are shown by the radius of curvature of the side wall of the part, the appearance of a radius of connection between the wall and the bottom of the part, as well as dimensional deviations that are expressed by the variation in the forming depth. Concerning the smoothness of the surfaces, it was observed that the best roughness results were obtained in the case of the TiN-coated tool.

| S-EPMC10573285 | biostudies-literature

OmicsDI is part of the ELIXIR infrastructure

OmicsDI is an Elixir interoperability service. Learn more ›

Tweets

OmicsDI Databases

PRIDE
PeptideAtlas
MassIVE
JPOST Repository
Physiome Model Repository

EGA
EVA
ENA
LINCS
PAXDB
Cell Collective

MetaboLights
Metabolomics Workbench
MetabolomeExpress
GNPS
BioModels
FAIRDOMHub

ArrayExpress
dbGaP
ExpressionAtlas
GEO
NODE

Information

Databases
Help
API
Contact us
Code on GitHub
Terms of use
Submit Data