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1,2-Bis(N'-benzoyl-thio-ureido)benzene.

ABSTRACT: The title compound, C(22)H(18)N(4)O(2)S(2), was characterized by (1)H and (13)C NMR, solid-state IR spectroscopy and X-ray crystallographic techniques. The crystal structure determination reveals that the twisting modes of the two side arms are different [C-N-C-O and C-N-C-N torsion angles = -1.2?(3) and 1.1?(3)°, respectively, in one arm and 24.1?(3) and -5.1?(3)°, respectively, in the other]. The crystal structure involves N-H?O and N-H?S hydrogen bonds.

SUBMITTER: Thiam EI

PROVIDER: S-EPMC2961338 | biostudies-literature | 2008 Apr

REPOSITORIES: biostudies-literature

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1,2-Bis(N'-benzoyl-thio-ureido)benzene.

Thiam Elhadj Ibrahima EI Diop Mayoro M Gaye Mohamed M Sall Abdou Salam AS Barry Aliou Hamady AH

Acta crystallographica. Section E, Structure reports online 20080402 Pt 5

The title compound, C(22)H(18)N(4)O(2)S(2), was characterized by (1)H and (13)C NMR, solid-state IR spectroscopy and X-ray crystallographic techniques. The crystal structure determination reveals that the twisting modes of the two side arms are different [C-N-C-O and C-N-C-N torsion angles = -1.2 (3) and 1.1 (3)°, respectively, in one arm and 24.1 (3) and -5.1 (3)°, respectively, in the other]. The crystal structure involves N-H⋯O and N-H⋯S hydrogen bonds. ...[more]

PMID: 21202269

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