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Bis[5-(4-methoxy-benz-yl)furan-3-yl]methanone.

ABSTRACT: The title compound, C(25)H(22)O(5), was obtained by a dehydrogenative carbonyl-ation reaction. It crystallizes with one half-mol-ecule in the asymmetric unit. The mol-ecules have crystallographic C(2) symmetry and the two atoms of the carbonyl group are located on the rotation axis. The meth-oxy groups are coplanar with the benzene ring to which they are attached [C-C-O-C = 1.0?(6)°]. The two furan rings are inclined at 17.3?(3)° with respect to each other and the dihedral angle between the furan ring and the benzene ring is 75.83?(12)°. The crystal structure is stabilized by C-H?O hydrogen bonds.

SUBMITTER: Bolte M 

PROVIDER: S-EPMC2970307 | biostudies-literature | 2009 Sep

REPOSITORIES: biostudies-literature

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Bis[5-(4-methoxy-benz-yl)furan-3-yl]methanone.

Bolte Michael M   Schwarz Lothar L   Hashmi A Stephen K AS  

Acta crystallographica. Section E, Structure reports online 20090905 Pt 10

The title compound, C(25)H(22)O(5), was obtained by a dehydrogenative carbonyl-ation reaction. It crystallizes with one half-mol-ecule in the asymmetric unit. The mol-ecules have crystallographic C(2) symmetry and the two atoms of the carbonyl group are located on the rotation axis. The meth-oxy groups are coplanar with the benzene ring to which they are attached [C-C-O-C = 1.0 (6)°]. The two furan rings are inclined at 17.3 (3)° with respect to each other and the dihedral angle between the fura  ...[more]

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