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1-(3-Chloro-phen-yl)-3-(4-nitro-phen-yl)urea.

ABSTRACT: In the title compound, C(13)H(10)ClN(3)O(3), prepared by the reaction of 1-chloro-3-isocyanato-benzene with 4-nitro-benzenamine, the two substituent benzene rings are roughly coplanar [inter-ring dihedral angle = 8.70?(7)°]. In the crystal, mol-ecules make cyclic inter-molecular associations through two urea-nitro N-H?O hydrogen bonds, forming a chain structure [give chain direction] in which there are also weak inter-molecular C-H?Cl inter-actions. The urea O atom has only intra-molecular aromatic ring C-H?O associations.

SUBMITTER: Sun T 

PROVIDER: S-EPMC3009072 | biostudies-literature | 2010 Oct

REPOSITORIES: biostudies-literature

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1-(3-Chloro-phen-yl)-3-(4-nitro-phen-yl)urea.

Sun Ting T   Li Jing J   Yang Feng-Ling FL  

Acta crystallographica. Section E, Structure reports online 20101013 Pt 11

In the title compound, C(13)H(10)ClN(3)O(3), prepared by the reaction of 1-chloro-3-isocyanato-benzene with 4-nitro-benzenamine, the two substituent benzene rings are roughly coplanar [inter-ring dihedral angle = 8.70 (7)°]. In the crystal, mol-ecules make cyclic inter-molecular associations through two urea-nitro N-H⋯O hydrogen bonds, forming a chain structure [give chain direction] in which there are also weak inter-molecular C-H⋯Cl inter-actions. The urea O atom has only intra-molecular aroma  ...[more]

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