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1,5-Bis(2-meth-oxy-benzyl-idene)thio-carbonohydrazide methanol monosolvate.

ABSTRACT: The title compound, C17H18N4O2S·CH3OH, was synthesized by the condensation reaction of o-meth-oxy-benzaldehyde with thio-carbohydrazide in methanol. The two benzene rings are inclined each to other at 31.7?(1)°. Inter-molecular N-H?O and bifurcated O-H?N(S) hydrogen bonds link two thio-carbonohydrazide and two solvent mol-ecules into a centrosymmetric unit. These units, related by translation along the b axis, are further aggregated into columns through N-H?S hydrogen bonds.

SUBMITTER: Yu J

PROVIDER: S-EPMC3770410 | biostudies-literature | 2013

REPOSITORIES: biostudies-literature

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1,5-Bis(2-meth-oxy-benzyl-idene)thio-carbonohydrazide methanol monosolvate.

Yu Jianfeng J Tang Shiming S Zeng Jingbin J Yan Zifeng Z

Acta crystallographica. Section E, Structure reports online 20130622 Pt 7

The title compound, C17H18N4O2S·CH3OH, was synthesized by the condensation reaction of o-meth-oxy-benzaldehyde with thio-carbohydrazide in methanol. The two benzene rings are inclined each to other at 31.7 (1)°. Inter-molecular N-H⋯O and bifurcated O-H⋯N(S) hydrogen bonds link two thio-carbonohydrazide and two solvent mol-ecules into a centrosymmetric unit. These units, related by translation along the b axis, are further aggregated into columns through N-H⋯S hydrogen bonds. ...[more]

PMID: 24046695

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