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Crystal structure of N-(quinolin-6-yl)hydroxyl-amine.

ABSTRACT: The title compound, C9H8N2O, crystallized with four independent mol-ecules in the asymmetric unit. The four mol-ecules are linked via one O-H?N and two N-H?N hydrogen bonds, forming a tetra-mer-like unit. In the crystal, mol-ecules are further linked by O-H?N and N-H?O hydrogen bonds forming layers parallel to (001). These layers are linked via C-H?O hydrogen bonds and a number of weak C-H?? inter-actions, forming a three-dimensional structure. The crystal was refined as a non-merohedral twin with a minor twin component of 0.319.

SUBMITTER: Rajapakse A 

PROVIDER: S-EPMC4257318 | biostudies-literature | 2014 Nov

REPOSITORIES: biostudies-literature

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Crystal structure of N-(quinolin-6-yl)hydroxyl-amine.

Rajapakse Anuruddha A   Hillebrand Roman R   Lewis Sarah M SM   Parsons Zachary D ZD   Barnes Charles L CL   Gates Kent S KS  

Acta crystallographica. Section E, Structure reports online 20141011 Pt 11

The title compound, C9H8N2O, crystallized with four independent mol-ecules in the asymmetric unit. The four mol-ecules are linked via one O-H⋯N and two N-H⋯N hydrogen bonds, forming a tetra-mer-like unit. In the crystal, mol-ecules are further linked by O-H⋯N and N-H⋯O hydrogen bonds forming layers parallel to (001). These layers are linked via C-H⋯O hydrogen bonds and a number of weak C-H⋯π inter-actions, forming a three-dimensional structure. The crystal was refined as a non-merohedral twin wi  ...[more]

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