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Crystal structure of 2,2-dimethyl-N-(pyridin-3-yl)propanamide.

ABSTRACT: In the title compound, C10H14N2O, the pyridine ring is inclined to the mean plane of the amide moiety [N-C(=O)C] by 17.60?(8)°. There is an intra-molecular C-H?O hydrogen bond present involving the carbonyl O atom. In the crystal, mol-ecules are linked via N-H?N hydrogen bonds, forming chains propagating along [100]. The tert-butyl group is disordered over two sets of sites with a refined occupancy ratio of 0.758?(12):0.242?(12).

SUBMITTER: El-Hiti GA

PROVIDER: S-EPMC4438820 | biostudies-other | 2015 Apr

REPOSITORIES: biostudies-other

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Crystal structure of 2,2-dimethyl-N-(pyridin-3-yl)propanamide.

El-Hiti Gamal A GA Smith Keith K Hegazy Amany S AS Alanazi Saud A SA Kariuki Benson M BM

Acta crystallographica. Section E, Crystallographic communications 20150321 Pt 4

In the title compound, C10H14N2O, the pyridine ring is inclined to the mean plane of the amide moiety [N-C(=O)C] by 17.60 (8)°. There is an intra-molecular C-H⋯O hydrogen bond present involving the carbonyl O atom. In the crystal, mol-ecules are linked via N-H⋯N hydrogen bonds, forming chains propagating along [100]. The tert-butyl group is disordered over two sets of sites with a refined occupancy ratio of 0.758 (12):0.242 (12). ...[more]

PMID: 26029437

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