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(Z)-3-[2-(2,4-Di-nitro-phen-yl)hydrazin-1-yl-idene]isobenzo-furan-1(3H)-one di-chloro-methane hemisolvate.

ABSTRACT: In the title compound, 2C14H8N4O6·CH2Cl2, the di-chloro-methane solvent mol-ecule resides on a crystallographic twofold axis. The mean plane of the phthaliso-imide ring is oriented at a dihedral angle of 32.93?(12)° with respect to the nitro-substituted benzene ring. An intra-molecular N-H?O hydrogen bond occurs. The crystal packing features a short Cl?O halogen-bond inter-action [3.093?(3)?Å].

SUBMITTER: Agarwal P

PROVIDER: S-EPMC3998610 | biostudies-literature | 2014 Apr

REPOSITORIES: biostudies-literature

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(Z)-3-[2-(2,4-Di-nitro-phen-yl)hydrazin-1-yl-idene]isobenzo-furan-1(3H)-one di-chloro-methane hemisolvate.

Agarwal Palak P Mishra Pragati P Gupta Nikita N Neelam Sahoo Priyaranjan P Kumar Satish S

Acta crystallographica. Section E, Structure reports online 20140312 Pt 4

In the title compound, 2C14H8N4O6·CH2Cl2, the di-chloro-methane solvent mol-ecule resides on a crystallographic twofold axis. The mean plane of the phthaliso-imide ring is oriented at a dihedral angle of 32.93 (12)° with respect to the nitro-substituted benzene ring. An intra-molecular N-H⋯O hydrogen bond occurs. The crystal packing features a short Cl⋯O halogen-bond inter-action [3.093 (3) Å]. ...[more]

PMID: 24826131

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